Hydrochloric Acid → HCID 57165760, compound

Participants

Reaction Steps

3.20 g of this (2R, 4R)-2-ethoxy-4-benzyloxypentane was dissolved in 50 ml of ethanol. 0.30 g of 0% palladium-carbon and 5 ml of 1 N hydrochloric acid were added, and hydrogenation was carried out at the room temperature at the atmospheric pressure. The catalyst was removed by filtration. The filtrate was concentrated. The residue was subjected to column chromatography (silica gel, developing solvent=chloroform) to obtain 0.91 g of (2R, 4R)-4-ethoxy-2pentanol.

Provenance & Evidence