HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 2-Propoxymethyl-4(3H)-pteridinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Aminopyrazine carboxamide | HCID 280292 | — |
| Product | 2-Propoxymethyl-4(3H)-pteridinone | HCID 135528321 | — |
Reaction Steps
Obtained using the procedure described in Example 1, starting with 4.6 g (0.033 mole) of 3-amino-2-pyrazinecarboxamide, 29.3 g (0.133 mole) of triethyl orthopropoxyacetate and 30 ml of acetic anhydride. Yld: 2.6 g (36%), m.p. 158°-160° C. (ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05167949 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-3e6845dffdc445588d6aa754abab3730 |
| Source note | uspto-grants-1992_12 |