HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Phenoxyethanimidamide → 4-Amino-2-(phenoxymethyl)pteridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Phenoxyethanimidamide | HCID 290245 | — |
| Edukt | 3-Aminopyrazine-2-carbonitrile | HCID 817699 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 4-Amino-2-(phenoxymethyl)pteridine | HCID 10634626 | — |
Reaktionsschritte
Obtained using the procedure described in section c of Example 2, starting with 3.0 g (0.025 mole) of 3-amino-2-pyrazinecarbonitrile and 3.8 g (0.025 mole) of 2-phenoxyacetamidine [prepared according to C. Djerassi and C. R. Scholz, J. Am. Chem. Soc. 1947, 69, 1688] in 100 ml of absolute ethanol. Refluxing time: 4 hours. Yld: 5.4 g (85%), m.p. 202°-204° C. (ethanol).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05167949 |
| Quelldatensatz | uspto-grants-1992_12 |
| ORD ID | ord-d6a5238402004c68a03e45fcc6a51194 |
| Quellennotiz | uspto-grants-1992_12 |