HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 2-(2,2,2-trifluoroethoxy)acetimidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 2-(2,2,2-Trifluoroethoxy)acetonitrile | HCID 14880147 | — |
| Product | Methyl 2-(2,2,2-trifluoroethoxy)acetimidate | HCID 14880139 | — |
Reaction Steps
Obtained using the procedure described in section a of Example 2, starting with 19.6 g (0.141 mole) of (2,2,2-trifluoroethoxy)acetonitrile and 0.3 g (0.013 gram-atom) of sodium in 95 ml of methanol. Reaction time: 24 hours. Yld: 15.6 g (65%), b.p.15 44°-47° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05167949 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-972c31eb90d243a9b52d0a8b5d25cc88 |
| Source note | uspto-grants-1992_12 |