HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 2-(2,2,2-Trifluoroethoxy)acetamidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methyl 2-(2,2,2-trifluoroethoxy)acetimidate | HCID 14880139 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(2,2,2-Trifluoroethoxy)acetamidine | HCID 10583013 | — |
Reaction Steps
Obtained using the procedure described in section b of Example 2, starting with 15.6 g (0.091 mole) of methyl 2-(2,2,2-trifluoroethoxy)acetimidate and 7.7 g (0.455 mole) of ammonia in 225 ml of absolute ethanol. Reaction time: 24 hours. Yld: 14.2 g (quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05167949 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-13c5a88875b247698acfadd4be84f8e2 |
| Source note | uspto-grants-1992_12 |