Ammonia → HCID 10729349, compound

HRID 1681046Notes

Reaction equation

HRID 1681046 reaction equation
[C:1]([C:4]1[CH:16]=[CH:15][C:7]([O:8][CH2:9][C:10](=[NH:14])OCC)=[C:6]([CH2:17][CH2:18][CH3:19])[C:5]=1[OH:20])(=[O:3])[CH3:2].[NH3:21]>C(O)C>[C:1]([C:4]1[CH:16]=[CH:15][C:7]([O:8][CH2:9][C:10]([NH2:14])=[NH:21])=[C:6]([CH2:17][CH2:18][CH3:19])[C:5]=1[OH:20])(=[O:3])[CH3:2]

Participants

4

Procedure

Obtained using the procedure described in section b of Example 17, starting with 25.0 g (0.0895 mole) of ethyl 2-(4-acetyl-3-hydroxy-2-propylphenoxy)acetimidate and 7.6 g (0.45 mole) of ammonia in 300 ml of absolute ethanol.

Workup

  1. customObtained

Sources & evidence

ORD record
ord-884de5cbeeff42e4b283986cedcd8d67
Source dataset
uspto-grants-1992_12
Patent number
US05167949

Reaction notes

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