HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 2-tert.-butyl-4-chloro-5-[4-(2,2-dichloroethenyl)-benzylthio]-3(2H)-pyridazinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Chloro-2-(1,1-dimethylethyl)-5-mercapto-3(2H)-pyridazinone | HCID 13469242 | — |
| Reactant | 4-(2,2-Dichloroethenyl)-benzyl bromide | HCID 19807204 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-tert.-butyl-4-chloro-5-[4-(2,2-dichloroethenyl)-benzylthio]-3(2H)-pyridazinone | HCID 19807201 | — |
Reaction Steps
1.2 g of 4-(2,2-dichloroethenyl)-benzyl bromide and 0.8 g of 2-tert.-butyl-4-chloro-5-mercapto-3(2H)-pyridazinone are added to a suspension of 0.7 g of potassium carbonate in 10 cc of dimethylformamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05169848 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-b8abd45db56c472588ab5bc44cd65549 |
| Source note | uspto-grants-1992_12 |