HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 86744711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Isobutyraldehyde | HCID 6561 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Ethyl isobutyrylacetate | HCID 81583 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 86744711 | HCID 86744711 | — |
Reaction Steps
158 g (1 mol) of ethyl isobutyrylacetate, 108 g (1.5 mol) of isobutyraldehyde, 8.75 ml of piperidine and 6.25 ml of acetic acid are stirred at 50° C. for 20 h in 400 ml of isopropanol. Volatile components are stripped off in a water pump vacuum and the residue is subsequently distilled in a high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05169857 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-390fe99c09844955b9630e028b599af7 |
| Source note | uspto-grants-1992_12 |