HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 19805835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 18995501 | HCID 18995501 | — |
| Product | HCID 19805835 | HCID 19805835 | — |
Reaction Steps
A solution of 2-(4-carboxyphenyl)-5-n-nonyl-1,3-dioxane (2.00 g) in thionyl chloride (10 g) was heated under refluxing for 4 hours with a small amount of N,N-dimethylformamide. Excessive amount of thionyl chloride was distilled to obtain the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05171471 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-77cb11c3bf8c4ffa92bd0c137d866870 |
| Source note | uspto-grants-1992_12 |