HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 53779739, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | HCID 19806300 | HCID 19806300 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53779739 | HCID 53779739 | 89% |
Reaction Steps
Dissolved in 10 ml of ethanol was 1.00 g (4.09 mmol) of 2-(2-aminoethylthio)-5-chlorobenzothiazole, and 0.36 ml (4.55 mmol) of ethyl isocyanate were added to the solution, which was stirred at room temperature for 15 minutes. The precipitated white crystals were then filtered out to obtain 1.15 g of the title compound (89% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05171746 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-daec018989a84509bab0689c9dd479b1 |
| Source note | uspto-grants-1992_12 |