Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Furfurylamine | HCID 3438 | — |
| Reactant | (R,R)-Stilbene oxide | HCID 185583 | — |
| Product | HCID 19806405 | HCID 19806405 | 78.4% |
Reaction Steps
A mixture of trans-stilbene oxide (1.96 g, 0.010 mol) and furfurylamine (3.00 g, 0.030 mol) was heated at 140° C. for 6 hours, and then allowed to stand at ambient temperature for 14 hours. The solidified reaction mixture was triturated with petroleum ether and the crude solid collected by filtration. Recrystallization from toluene-isooctane gave 2.3 g (78%) of the product; mp 141°-144° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05171753 |
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| Source dataset | uspto-grants-1992_12 |
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| ORD ID | ord-3ad3ef8ec2f5425e81b53135b5b01e5c |
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| Source note | uspto-grants-1992_12 |
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