Diglycolamine → HCID 19806392, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of trans-stilbene oxide (1.96 g, 0.010 mol) and 2-(2-aminoethoxy)ethanol (3.05 g, 0.030 mol) was heated at 140° C. for 6 hours. After standing at room temperature for 14 hours the reaction mixture was triturated with water, the solid product collected, and dried under ambient conditions for 3 days to obtain 2.77 g (92%) of material. The solid was recrystallized from methanol-isopropyl ether to obtain 1.89 g of the product; mp 140°-142° C.

Provenance & Evidence