HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1681355Generated: November 3, 2026
(2-(Methylthio)ethyl)amine → HCID 19806393, compound
https://huagongshe.com/reaction/1681355
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | (2-(Methylthio)ethyl)amine | HCID 87697 | — |
| Reactant | (R,R)-Stilbene oxide | HCID 185583 | — |
| Reactant | Diisopropylether methanol | HCID 21882575 | — |
| Product | HCID 19806393 | HCID 19806393 | 67% |
Reaction Steps
A mixture of trans-stilbene oxide (1.18 g, 0.006 mol) and 2-(methylthio)ethylamine (0.78 g, 0.0085 mol) was heated at 140° C. in an oil bath for 15 hours. The cooled solid reaction mixture was triturated with isooctane and the red-brown solid collected. This was triturated with methanol-isopropyl ether giving an off-white solid (1.15 g, 67% yield); mp 163°-165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05171753 |
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| Source dataset | uspto-grants-1992_12 |
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| ORD ID | ord-375e2a17aa3d4b43a53c3e451b858803 |
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| Source note | uspto-grants-1992_12 |
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