HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylimidazole → HCID 13810558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylimidazole | HCID 12749 | — |
| Reactant | HCID 11161699 | HCID 11161699 | — |
| Product | HCID 13810558 | HCID 13810558 | — |
Reaction Steps
Combine 100 g (0.36 mol) of N-[(4-chloro-1-oxobutyl)phenyl]methanesulfonamide with 400 g (4.88 mol) of 2-methylimidazole and heat to 175° C. for 22 hr under argon. Crystallization from methylene chloride provides the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05171859 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-7dc4e5d00c9c4904a835825e247803b7 |
| Source note | uspto-grants-1992_12 |