HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylimidazole → HCID 19806643, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylimidazole | HCID 12749 | — |
| Reactant | Cyclopropyl(3,4-dichlorophenyl)methanone | HCID 19806646 | — |
| Product | HCID 19806643 | HCID 19806643 | — |
Reaction Steps
Combine 10 g (46.5 mmol) of cyclopropyl-(3,4-dichlorophenyl)methanone with 20 g (0.24 mol) of 2-methylimidazole and heat to 175° C. under nitrogen for 70 hr. The title compound is isolated by column chromatography on silica gel using methylene chloride as the solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05171859 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-6477dfecd5bd4760b1da0a914df33b26 |
| Source note | uspto-grants-1992_12 |