Cyanuric chloride → HCID 21468019, compound

Participants

Reaction Conditions

Reaction Steps

A solution of 118.20 g (0.30 mol) of N,N'-bis(2,2,6,6-tetramethyl-4-piperidyl)-1,6-diaminohexane in 150 ml of 1,2-dichloroethane is added slowly in the course of 2 hours to a solution, maintained at 0° C., containing 110.70 g (0.60 mol) of cyanuric chloride in 800 ml of 1,2-dichloroethane. 250 ml of an aqueous solution containing 25.20 g (0.63 mol) of sodium hydroxide are then added in 30 minutes at 0° C., and stirring is continued for 2 hours at 0° C. The aqueous phase is then separated off, the organic phase is washed repeatedly with water and dehydrated by means of anhydrous sodium sulfate, and a white solid of melting point 161°-163° C. is precipitated by evaporation of the solvent.

Provenance & Evidence