HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 19382165, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 5-Benzyl-1-oxa-5-azaspiro[2.4]heptane | HCID 11194805 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19382165 | HCID 19382165 | — |
Reaction Steps
26.8 g (0.14 mol) of 5-benzyl-1-oxa-5-azaspiro[2,4]heptane are heated overnight under reflux with 2.6 ml (14 mmol) of 30% strength sodium methoxide solution in 200 ml of absolute methanol. The product is concentrated and distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05173484 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-01673de67287477c8370d78d09030785 |
| Source note | uspto-grants-1992_12 |