HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → 9-Octadecenal, (9Z)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Oleyl Alcohol | HCID 5284499 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 9-Octadecenal, (9Z)- | HCID 5364492 | 90.1% |
Reaction Steps
An 18 g portion of pyridinium chlorochromate was slurried in 200 ml of dichloromethane. A solution of 15 g of oleyl alcohol in 200 ml of dichloromethane was added. This mixture was stirred for 4 hours, then poured into ether and filtered through hydrous magnesium silicate. The filtrate was evaporated, giving 13.42 g of the desired compound as a colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05173510 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-3da8471e31c1456c88556b8f0d3fc364 |
| Source note | uspto-grants-1992_12 |