1-Chloromethyl-2-methylnaphthalene → HCID 67918269, compound

HRID 1682057Notes

Reaction equation

HRID 1682057 reaction equation
[NH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]1[CH2:7][CH2:8][N:9]1[C:15](=[O:16])[CH2:14][C:13]2[CH:17]=[C:18]([O:23][CH3:24])[C:19]([O:21][CH3:22])=[CH:20][C:12]=2[CH2:11][CH2:10]1.[Cl:25][CH2:26][C:27]1[C:36]2[C:31](=[CH:32][CH:33]=[CH:34][CH:35]=2)[CH:30]=[CH:29][C:28]=1[CH3:37]>>[ClH:25].[CH3:37][C:28]1[CH:29]=[CH:30][C:31]2[C:36](=[CH:35][CH:34]=[CH:33][CH:32]=2)[C:27]=1[CH2:26][N:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]1[CH2:7][CH2:8][N:9]1[C:15](=[O:16])[CH2:14][C:13]2[CH:17]=[C:18]([O:23][CH3:24])[C:19]([O:21][CH3:22])=[CH:20][C:12]=2[CH2:11][CH2:10]1

Participants

3

Reactant 2

HCID 811061-Chloromethyl-2-methylnaphthaleneHCID 19803848HCID 19803848, compound

Product 1

HCID 67918269HCID 67918269, compound

Procedure

Prepared from 3-[2-(piperid-2-yl)-ethyl]-7,8-dimethoxy-2-oxo-1,3,4,5-tetrahydro-2H-3-benzazepine and 1-chloromethyl-2-methyl-naphthalene analogously to Example 1.

Sources & evidence

ORD record
ord-2a2495a78d4640f28637457acb1816e1
Source dataset
uspto-grants-1992_12
Patent number
US05175157

Reaction notes

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