HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl nitroacetate → HCID 59896635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl nitroacetate | HCID 69379 | — |
| Reactant | HCID 22450336 | HCID 22450336 | — |
| Product | HCID 59896635 | HCID 59896635 | 57.3% |
Reaction Steps
A mixture of 1.4 g (0.0061 mole) of S-methyl-N-(6-chloro-3-pyridylmethyl)-N'-methylisothiourea obtained in Example 64 (2) and 2.7 g of ethyl nitroacetate was stirred with heating at 75°-80° C. for 3 hours. After cooling, the crystals were collected by filtration, washed with CH3CN and dried. The procedure gave 1.1 g of the title compound as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05175301 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-27c0d30a67ef4d62b556527ca8a1f36e |
| Source note | uspto-grants-1992_12 |