Nonanoyl chloride → N-Nonanoyl-3,3-dichlorocaprolactam

HRID 1682382Notes

Reaction equation

[C:1]([N:9]1[CH2:15][CH2:14][CH2:13][C:12]([Cl:17])([Cl:16])[CH2:11][C:10]1=[O:18])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:19](Cl)(=O)[CH2:20]CCCCCCC>>[C:1]([N:9]1[CH2:15][CH2:14][CH2:13][C:12]([Cl:16])([Cl:17])[CH2:11][C:10]1=[O:18])(=[O:8])[CH2:2][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:19][CH3:20]

Participants

Reactant 2

HCID 69819Nonanoyl chloride

HCID 19043813N-Benzoyl-3,3-dichlorocaprolactam

Product 1

HCID 19043818N-Nonanoyl-3,3-dichlorocaprolactam

Procedure

Synthesized as for N-benzoyl-3,3-chlorocaprolactam (Example IX) using nonanoyl chloride (Aldrich) in place of benzoyl chloride.

Sources & evidence

ORD record: ord-2fd26fc6bf254b9c95159f8e4ee5ae47
Source dataset: uspto-grants-1997_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05635103

Reaction notes

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