4-Nitrobenzoyl chloride → N-(4-Nitrobenzoyl)-3-chlorocaprolactam

HRID 1682383Notes

Reaction equation

HRID 1682383 reaction equation
[C:1]([N:9]1[CH2:15][CH2:14][CH2:13][CH:12]([Cl:16])[CH2:11][C:10]1=[O:17])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[N+:18](C1C=CC(C(Cl)=O)=CC=1)([O-:20])=[O:19]>>[N+:18]([C:5]1[CH:4]=[CH:3][C:2]([C:1]([N:9]2[CH2:15][CH2:14][CH2:13][CH:12]([Cl:16])[CH2:11][C:10]2=[O:17])=[O:8])=[CH:7][CH:6]=1)([O-:20])=[O:19]

Participants

3

Reactant 2

HCID 85024-Nitrobenzoyl chlorideHCID 190438231-Benzoyl-4-chloroazepan-2-one

Product 1

HCID 19043819N-(4-Nitrobenzoyl)-3-chlorocaprolactam

Procedure

Synthesized as in the alternative preparation for N-benzoyl-3-chlorocaprolactam (Example VI) using 4-nitrobenzoyl chloride in place of benzoyl chloride.

Sources & evidence

ORD record
ord-1d40338d5ae2483381f46eae59008434
Source dataset
uspto-grants-1997_06
Patent number
US05635103

Reaction notes

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