HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Piperidone → 3-Chlorovalerolactam
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Piperidone | HCID 12665 | — |
| Reactant | 3-Chlorovalerolactam | HCID 19043820 | — |
| Reactant | 1-Benzoyl-4-chloroazepan-2-one | HCID 19043823 | — |
| Reactant | 3-Chlorocaprolactam | HCID 19369318 | — |
| Product | 3-Chlorovalerolactam | HCID 19043820 | — |
| Product | N-Benzoyl-3-chlorovalerolactam | HCID 19043826 | — |
Reaction Steps
3-Chlorovalerolactam is synthesized as for 3-chlorocaprolactam (prepared from caprolactam according to J. Am. Chem. Soc. 1958, 80, 6238) using valerolactam in place of caprolactam. Thereafter, the title compound is synthesized as for N-benzoyl-3-chlorocaprolactam (Example VI) using 3-chlorovalerolactam in place of 3-chlorocaprolactam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05635103 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-dbb5d49f3f304609adcf883a27cfe5f5 |
| Source note | uspto-grants-1997_06 |