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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1682742Generated: November 4, 2026

Potassium Carbonate → HCID 21832140, compound

https://huagongshe.com/reaction/1682742

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantBromoacetoneHCID 11715—
ReactantMethyl 3-HydroxyphenylacetateHCID 39129—
SolventDimethylformamideHCID 6228—
ProductHCID 21832140HCID 21832140—

Reaction Steps

Following a procedure similar to that described in Preparation 3, but using 2.8 g of methyl 3-hydroxyphenylacetate, 3.5 g of bromoacetone, 4 g of potassium carbonate and 30 ml of dimethylformamide, the title compound was obtained having an Rf=0.41 (thin layer chromatography over silica gel, using a 2:5 by volume mixture of ethyl acetate and hexane as the developing solvent).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05635534
Source datasetuspto-grants-1997_06
ORD IDord-3c23668291fa4b18911c6e70e1af3715
Source noteuspto-grants-1997_06