HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21832140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Bromoacetone | HCID 11715 | — |
| Reactant | Methyl 3-Hydroxyphenylacetate | HCID 39129 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21832140 | HCID 21832140 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 3, but using 2.8 g of methyl 3-hydroxyphenylacetate, 3.5 g of bromoacetone, 4 g of potassium carbonate and 30 ml of dimethylformamide, the title compound was obtained having an Rf=0.41 (thin layer chromatography over silica gel, using a 2:5 by volume mixture of ethyl acetate and hexane as the developing solvent).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05635534 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-3c23668291fa4b18911c6e70e1af3715 |
| Source note | uspto-grants-1997_06 |