HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 22872083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 53993388 | HCID 53993388 | — |
| Product | HCID 22872083 | HCID 22872083 | — |
Reaction Steps
A 200 mg portion of (4aR)-(10bR)-10b-methyl-8-(phenylsulfonyl)-1,2,3,4,4a,5,6,10b-octahydrobenzo[f]-quinolin-3-one was methylated with methyl iodide to obtain 144 mg of the desired product. mp 165°-167° FDMS: m/e=369. α[D]589 =+76.2, α[D]365 =+269.7 (chloroform).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05635197 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-50860fa6edb04602afd7a5ccfc64ce11 |
| Source note | uspto-grants-1997_06 |