HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetylene → HCID 44351848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetylene | HCID 10821 | — |
| Reactant | (4aR)-(10bR)-4,10b-dimethyl-8-bromo-1,2,3,4,4a,5,6,10b-octahydrobenzo[f]quinolin-3-one | HCID 15355317 | — |
| Product | HCID 44351848 | HCID 44351848 | — |
Reaction Steps
A 1 g portion of (4aR)-(10bR)-4,10b-dimethyl-8-bromo-1,2,3,4,4a,5,6,10b-octahydrobenzo[f]quinolin-3-one was reacted with 0.4 mL of phenylacetylene in a process substantially similar to that of Example 281 to obtain the desired title product in pure form. mp 205°-208°; FDMS 329.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05635197 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-0ae915a54d384084a6940cd3b36a322e |
| Source note | uspto-grants-1997_06 |