Benzoyl chloride, 3,4,5-trimethoxy- → HCID 18333504, compound

HRID 1682988Notes

Reaction equation

HRID 1682988 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]3([CH2:15][CH2:16][OH:17])[CH2:14][CH2:13][NH:12][CH2:11]3)=[CH:9][C:4]=2[O:3][CH2:2]1.[CH3:18][O:19][C:20]1[CH:21]=[C:22]([CH:26]=[C:27]([O:31][CH3:32])[C:28]=1[O:29][CH3:30])[C:23](Cl)=[O:24]>>[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]3([CH2:15][CH2:16][OH:17])[CH2:14][CH2:13][N:12]([C:23](=[O:24])[C:22]4[CH:21]=[C:20]([O:19][CH3:18])[C:28]([O:29][CH3:30])=[C:27]([O:31][CH3:32])[CH:26]=4)[CH2:11]3)=[CH:9][C:4]=2[O:3][CH2:2]1

Participants

3

Reactant 2

HCID 78282Benzoyl chloride, 3,4,5-trimethoxy-HCID 18333383HCID 18333383, compound

Product 1

HCID 18333504HCID 18333504, compound

Procedure

Prepare by the method of example 3.1 using 2-(3-benzo[1,3]dioxol-5-yl-pyrrolidin-3-yl)-ethanol (23 mmol) and 3,4,5-trimethoxy-benzoyl chloride (23 mmol). Chromatograph on silica gel to give the title compound.

Sources & evidence

ORD record
ord-b949d233dec64e059e4f8b15028bf2cc
Source dataset
uspto-grants-1997_06
Patent number
US05635510

Reaction notes

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