Ethyl bromoacetate → HCID 50896401, compound

HRID 1683057Notes

Reaction equation

[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][C:7]#[N:8].Br[CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12]>>[CH2:14]([O:13][C:11](=[O:12])[CH2:10][C:6]([C:7]#[N:8])([C:2]1[S:1][CH:5]=[CH:4][CH:3]=1)[CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])[CH3:15]

Participants

Reactant 2

HCID 7748Ethyl bromoacetate

HCID 728802-Thienylacetonitrile

Product 1

HCID 50896401HCID 50896401, compound

Procedure

Prepare by the method of example 1.1.2 using thiophen-2-yl-acetonitrile (0.161 mol) and ethyl bromoacetate (0.325 mol). Chromatograph on silica gel to give the title compound.

Sources & evidence

ORD record: ord-172f086b1a0648b9a40a90296810bf7f
Source dataset: uspto-grants-1997_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05635510

Reaction notes

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