(3,4-Dichlorophenyl)acetonitrile → HCID 15381168, compound

HRID 1683090Notes

Reaction equation

HRID 1683090 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH2:9][C:10]#[N:11])[CH:5]=[CH:6][C:7]=1[Cl:8].Br[CH2:13][CH2:14][CH2:15][O:16][CH:17]1[CH2:22][CH2:21][CH2:20][CH2:19][O:18]1>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]([CH2:13][CH2:14][CH2:15][O:16][CH:17]2[CH2:22][CH2:21][CH2:20][CH2:19][O:18]2)[C:10]#[N:11])[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

3

Reactant 2

HCID 76690(3,4-Dichlorophenyl)acetonitrileHCID 27779882-(3-Bromopropoxy)tetrahydro-2H-pyran

Product 1

HCID 15381168HCID 15381168, compound

Procedure

Prepare according to the method of example 11.1 using 3,4-dichlorophenylacetonitrile (50 mmol) and 2-(3-bromo-propoxy)-tetrahydro-pyran (50 mmol). Chromatograph on silica gel to give the title compound.

Workup

  1. customPrepare

Sources & evidence

ORD record
ord-dd8057d64d0142ecb3c277ecf9595a58
Source dataset
uspto-grants-1997_06
Patent number
US05635510

Reaction notes

Loading…