HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Acetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one → 1,8-Diacetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Acetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one | HCID 10353298 | — |
| Reactant | N-(8-Oxo-5,6,7,8-tetrahydronaphthalen-1-YL)acetamide | HCID 12119265 | — |
| Product | 1,8-Diacetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one | HCID 22449453 | — |
Reaction Steps
The reaction was carried out in the same manner as in Example 1-(2), except that 270 mg of the compound prepared in (2) above was used instead of 8-acetylamino-1-tetralone of Example 1-(2). The reaction mixture obtained by the post-treatment was further reacted in the same manner as in Example 1-(3) and post-treated to produce 126 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05637770 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-d903d02aa1584bc294ef4d6dab54644d |
| Source note | uspto-grants-1997_06 |