Sodium Hydroxide → HCID 69910131, compound

Participants

Reaction Conditions

Reaction Steps

A solution of 0.26 g (0.8 mmol) of bis(phenethyl) methyl phosphate in 3.2 mL of dry acetonitrile was stirred at 0° C. under N2 while 0.23 mL (2.18 eq.) of TMSBr was added dropwise. The solution was stirred at 0° C. for 1.5 hours. The solvent was removed and the residue was dissolved in NaOH (1.0 eq.) in MeOH solution. After 30 minutes at room temperature, the solution was concentrated, and the white solid was taken up in ether (6.0 mL) and filtered to give sodium bis(phenethyl) phosphate.

Provenance & Evidence