3,4-Diethoxybenzene-1-carbothioamide → HCID 19041047, compound

HRID 1683787Notes

Reaction equation

HRID 1683787 reaction equation
[N:1]1([C:6]2[N:11]=[C:10]([C:12](=O)[CH2:13]Br)[CH:9]=[CH:8][CH:7]=2)[CH:5]=[N:4][CH:3]=[N:2]1.[CH2:16]([O:18][C:19]1[CH:20]=[C:21]([CH:25]=[CH:26][C:27]=1[O:28][CH2:29][CH3:30])[C:22]([NH2:24])=[S:23])[CH3:17]>>[CH2:16]([O:18][C:19]1[CH:20]=[C:21]([C:22]2[S:23][CH:13]=[C:12]([C:10]3[CH:9]=[CH:8][CH:7]=[C:6]([N:1]4[CH:5]=[N:4][CH:3]=[N:2]4)[N:11]=3)[N:24]=2)[CH:25]=[CH:26][C:27]=1[O:28][CH2:29][CH3:30])[CH3:17]

Participants

3

Reactant 2

HCID 77452503,4-Diethoxybenzene-1-carbothioamideHCID 19041090HCID 19041090, compound

Product 1

HCID 19041047HCID 19041047, compound

Procedure

A reaction was conducted in the same manner as in Example 1, by using 6-(1,2,4-triazol-1-yl)-2-(α-bromoacetyl)pyridine and 3,4-diethoxythiobenzamide, to obtain 2-(3,4-diethoxyphenyl)-4-[6-(1,2,4-triazol-1-yl)-2-pyridyl]thiazole.

Sources & evidence

ORD record
ord-81f387b7ea31487684b5cc708748e087
Source dataset
uspto-grants-1997_06
Patent number
US05639770

Reaction notes

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