3,4-Diethoxybenzene-1-carbothioamide → HCID 19041113, compound

HRID 1683790Notes

Reaction equation

HRID 1683790 reaction equation
[C:1]([CH2:4][CH2:5][O:6][C:7]1[N:12]=[C:11]([C:13](=O)[CH2:14]Br)[CH:10]=[CH:9][CH:8]=1)([OH:3])=[O:2].[CH2:17]([O:19][C:20]1[CH:21]=[C:22]([CH:26]=[CH:27][C:28]=1[O:29][CH2:30][CH3:31])[C:23]([NH2:25])=[S:24])[CH3:18]>>[CH2:17]([O:19][C:20]1[CH:21]=[C:22]([C:23]2[S:24][CH:14]=[C:13]([C:11]3[CH:10]=[CH:9][CH:8]=[C:7]([O:6][CH2:5][CH2:4][C:1]([OH:3])=[O:2])[N:12]=3)[N:25]=2)[CH:26]=[CH:27][C:28]=1[O:29][CH2:30][CH3:31])[CH3:18]

Participants

3

Reactant 2

HCID 77452503,4-Diethoxybenzene-1-carbothioamideHCID 19041002HCID 19041002, compound

Product 1

HCID 19041113HCID 19041113, compound

Procedure

A reaction was conducted in the same manner as in Example 1, by using 6-(2-carboxyethoxy)-2-(α-bromoacetyl)pyridine and 3,4-diethoxythiobenzamide, to obtain 2-(3,4-diethoxyphenyl)-4-[6-(2-carboxyethoxy)-2-pyridyl]thiazole.

Sources & evidence

ORD record
ord-69a50ee9110c4cf1870ad258993d6915
Source dataset
uspto-grants-1997_06
Patent number
US05639770

Reaction notes

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