3,4-Diethoxybenzene-1-carbothioamide → HCID 19041040, compound

HRID 1683793Notes

Reaction equation

HRID 1683793 reaction equation
[OH:1][CH:2]([C:5]1[N:10]=[C:9]([C:11](=O)[CH2:12]Br)[CH:8]=[CH:7][CH:6]=1)[CH2:3][OH:4].[CH2:15]([O:17][C:18]1[CH:19]=[C:20]([CH:24]=[CH:25][C:26]=1[O:27][CH2:28][CH3:29])[C:21]([NH2:23])=[S:22])[CH3:16]>>[CH2:15]([O:17][C:18]1[CH:19]=[C:20]([C:21]2[S:22][CH:12]=[C:11]([C:9]3[CH:8]=[CH:7][CH:6]=[C:5]([CH:2]([OH:1])[CH2:3][OH:4])[N:10]=3)[N:23]=2)[CH:24]=[CH:25][C:26]=1[O:27][CH2:28][CH3:29])[CH3:16]

Participants

3

Reactant 2

HCID 77452503,4-Diethoxybenzene-1-carbothioamideHCID 19041007HCID 19041007, compound

Product 1

HCID 19041040HCID 19041040, compound

Procedure

A reaction was conducted in the same manner as in Example 1, by using 6-(1,2-dihydroxyethyl)-2-(α-bromoacetyl)pyridine and 3,4-diethoxythiobenzamide, to obtain 2-(3,4-diethoxyphenyl)-4-[6-(1,2-dihydroxyethyl)-2-pyridyl]thiazole.

Sources & evidence

ORD record
ord-d94a75bcede94d02a9917e1d57a1fe65
Source dataset
uspto-grants-1997_06
Patent number
US05639770

Reaction notes

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