Acetic Acid → HCID 19041519, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of dipropyl-(6,7,8,9-tetrahydro-3H-benzo[e]indol-7-yl)amine (200 mg, 0.74 mmol), water (5 ML) in acetic acid (50 mL) was added dropwise to a solution of pyridiniumhydrobromide perbromide (310 mg, 0.91 mmol) in acetic acid (100 mL). The solution was heated and stirred at 80° C. over night. After cooling the solution was evaporated to an aqueous residue, which was basified (10% sodium carbonate) and extracted three times with ethyl acetate. The organic extract was dried (magnesium sulfate), filtered and evaporated to yield 210 mg (100%) of the material.:

Provenance & Evidence