HCID 131720048, compound → HCID 54169137, compound

Participants

Reaction Steps

To a solution of alcohol from Step 2 (293 mg) in CH2Cl2 (12 mL) was added a mixture of pyridinium chlorochromate (542 mg, 1.5 eq) and celite (542 mg). The suspension was stirred at r.t. overnight, and allowed to settle. The supernatant was collected and evaporated down to a residue which was chromatographed on silica gel, eluting with a 1:2 mixtue of EtOAc and hexane, to afford the desired ketone as a colorless liquid (189 mg).

Provenance & Evidence