HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → Methylsulfinylmethylbenzylmethyl sulfonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Methylmethylsulfinylmethyl sulfide | HCID 54140058 | — |
| Product | Methylsulfinylmethylbenzylmethyl sulfonium bromide | HCID 86750971 | 26% |
Reaction Steps
6.21 g of methylmethylsulfinylmethyl sulfide and 17.10 g of benzyl bromide were mixed, and were then allowed to stand in reaction at 50° C. for five months. The compound obtained was washed with ether, dried at 40° C. under reduced pressure, affording a precursor, methylsulfinylmethylbenzylmethyl sulfonium bromide. Yield: 26%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05639903 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-7da4a01399a347dda8cd25e19cffa251 |
| Source note | uspto-grants-1997_06 |