HuagongsheHuagongshe Chemistry Print Report · For research reference only
6,7-Dimethoxy-1,2,3,4-Tetrahydroisoquinoline → HCID 10769927, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6,7-Dimethoxy-1,2,3,4-Tetrahydroisoquinoline | HCID 15623 | — |
| Reactant | HCID 19042100 | HCID 19042100 | — |
| Product | HCID 10769927 | HCID 10769927 | 41.1% |
Reaction Steps
The procedure of Example 3 is repeated using 0.836 g of α-(5-bromooctyl)-3,4-dimethoxy-α-[(4-methylphenyl)thio]benzeneacetonitrile and 0.675 g of 6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline. This affords 0.422 g of the desired product as a brown gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05639887 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-36fd9b6c3c9d41b8905a4a7b9bb4d88d |
| Source note | uspto-grants-1997_06 |