HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,5-Dibromopentane → HCID 10812778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,5-Dibromopentane | HCID 8100 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 10541200 | HCID 10541200 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 10812778 | HCID 10812778 | 81.5% |
Reaction Steps
The title compound is prepared by the procedure of Example 113 using 1.3 g of product from Example 117, 0.218 g of 50% sodium hydride, 2.15 g of 1,5-dibromopentane and 16 ml of dimethyl sulfoxide to give after chromatography 1.61 g of the desired product as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05639887 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-447c86ab876a487eb738d4625a1b8777 |
| Source note | uspto-grants-1997_06 |