1-Bromoheptane → HCID 178444226, compound
Reaction equation
[CH2:1](Br)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[F:9][C:10]1[CH:11]=[C:12]([O:18][CH2:19][CH:20]2[CH2:25][CH2:24][SiH:23](Cl)[CH2:22][CH2:21]2)[CH:13]=[C:14]([F:17])[C:15]=1[F:16]>>[F:17][C:14]1[CH:13]=[C:12]([O:18][CH2:19][C@H:20]2[CH2:21][CH2:22][Si@H:23]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7])[CH2:24][CH2:25]2)[CH:11]=[C:10]([F:9])[C:15]=1[F:16]Participants
3
Procedure
The general procedure of Example 1 was repeated using n-heptyl bromide and 4-(3,4,5-trifluorophenyloxymethyl)-1-chloro-1-silacyclohexane, thereby obtaining the intended product.
Workup
- customobtaining the intended product
Sources & evidence
- ORD record
- ord-458fe62c2b464ebf89d9fcdffe661082
- Source dataset
- uspto-grants-1997_06
- Patent number
- US05641430
Reaction notes
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