1-Bromoheptane → HCID 178444222, compound
Reaction equation
[CH2:1](Br)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[Cl:9][C:10]1[CH:15]=[CH:14][C:13]([O:16][CH2:17][CH:18]2[CH2:23][CH2:22][SiH:21](Cl)[CH2:20][CH2:19]2)=[CH:12][C:11]=1[F:25]>>[Cl:9][C:10]1[CH:15]=[CH:14][C:13]([O:16][CH2:17][C@H:18]2[CH2:23][CH2:22][Si@H:21]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7])[CH2:20][CH2:19]2)=[CH:12][C:11]=1[F:25]Participants
3
Procedure
The general procedure of Example 1 was repeated using n-heptyl bromide and 4-(4-chloro-3-fluorophenyloxymethyl)-1-chloro-1-silacyclohexane, thereby obtaining the intended product.
Workup
- customobtaining the intended product
Sources & evidence
- ORD record
- ord-3d90eb0dc607435fb246ce2f45618e92
- Source dataset
- uspto-grants-1997_06
- Patent number
- US05641430
Reaction notes
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