1-Bromo-3-methylbutane → HCID 178447780, compound

HRID 1684451Notes

Reaction equation

HRID 1684451 reaction equation
[CH3:1][CH:2]([CH3:6])[CH2:3][CH2:4]Br.[Cl:7][C:8]1[C:13]([F:14])=[CH:12][C:11]([O:15][CH2:16][CH:17]2[CH2:22][CH2:21][SiH:20](Cl)[CH2:19][CH2:18]2)=[CH:10][C:9]=1[F:24]>>[Cl:7][C:8]1[C:13]([F:14])=[CH:12][C:11]([O:15][CH2:16][C@H:17]2[CH2:22][CH2:21][Si@H:20]([CH2:4][CH2:3][CH:2]([CH3:6])[CH3:1])[CH2:19][CH2:18]2)=[CH:10][C:9]=1[F:24]

Participants

3

Reactant 2

HCID 78911-Bromo-3-methylbutaneHCID 123280316HCID 123280316, compound

Product 1

HCID 178447780HCID 178447780, compound

Procedure

The general procedure of Example 1 was repeated using 3-methylbutyl bromide and 4-(4-chloro-3,5-difluorophenyloxymethyl)-1-chloro-1-silacyclohexane, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-7eaa1bcaadaf42a093ec78b706f292a4
Source dataset
uspto-grants-1997_06
Patent number
US05641430

Reaction notes

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