4-Ethoxy-2,3-difluorophenol → HCID 178444223, compound

HRID 1684454Notes

Reaction equation

HRID 1684454 reaction equation
[F:1][C:2]1[C:7]([F:8])=[C:6]([O:9][CH2:10][CH3:11])[CH:5]=[CH:4][C:3]=1[OH:12].Br[CH2:14][CH:15]1[CH2:20][CH2:19][Si:18]([CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH3:33])(C2C=CC=CC=2)[CH2:17][CH2:16]1>>[F:1][C:2]1[C:7]([F:8])=[C:6]([O:9][CH2:10][CH3:11])[CH:5]=[CH:4][C:3]=1[O:12][CH2:14][C@H:15]1[CH2:20][CH2:19][Si@H:18]([CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH3:33])[CH2:17][CH2:16]1

Participants

3

Reactant 2

HCID 144957634-Ethoxy-2,3-difluorophenolHCID 189357894-Bromomethyl-1-n-heptyl-1-phenyl-1-silacyclohexane

Product 1

HCID 178444223HCID 178444223, compound

Procedure

The general procedure of Example 9 was repeated using 2,3-difluoro-4-ethoxyphenol and 4-bromomethyl-1-n-heptyl-1-phenyl-1-silacyclohexane, thereby obtaining the intended compound.

Workup

  1. customobtaining the intended compound

Sources & evidence

ORD record
ord-9cf21c2c105241fc92d571a2f280e35b
Source dataset
uspto-grants-1997_06
Patent number
US05641430

Reaction notes

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