4-Chloro-2-fluorophenol → HCID 178444220, compound

HRID 1684457Notes

Reaction equation

HRID 1684457 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[C:4]([F:9])[CH:3]=1.Br[CH2:11][CH:12]1[CH2:17][CH2:16][Si:15]([CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])(C2C=CC=CC=2)[CH2:14][CH2:13]1>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH2:11][C@H:12]2[CH2:17][CH2:16][Si@H:15]([CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])[CH2:14][CH2:13]2)=[C:4]([F:9])[CH:3]=1

Participants

3

Reactant 2

HCID 1819754-Chloro-2-fluorophenolHCID 189357894-Bromomethyl-1-n-heptyl-1-phenyl-1-silacyclohexane

Product 1

HCID 178444220HCID 178444220, compound

Procedure

The general procedure of Example 9 was repeated using 4-chloro-2-fluorophenol and 4-bromomethyl-1-n-heptyl-1-phenyl-1-silacyclohexane, thereby obtaining the intended compound.

Workup

  1. customobtaining the intended compound

Sources & evidence

ORD record
ord-7a0e97fa464447128709f289c0218153
Source dataset
uspto-grants-1997_06
Patent number
US05641430

Reaction notes

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