3,4,5-Trifluorophenol → HCID 178461116, compound

HRID 1684460Notes

Reaction equation

HRID 1684460 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([OH:10])[CH:5]=[C:6]([F:9])[C:7]=1[F:8].Br[CH2:12][CH:13]1[CH2:18][CH2:17][Si:16]([CH2:25][CH2:26][CH2:27][CH:28]([F:30])[CH3:29])(C2C=CC=CC=2)[CH2:15][CH2:14]1>>[F:1][C:2]1[CH:3]=[C:4]([O:10][CH2:12][C@H:13]2[CH2:14][CH2:15][Si@H:16]([CH2:25][CH2:26][CH2:27][CH:28]([F:30])[CH3:29])[CH2:17][CH2:18]2)[CH:5]=[C:6]([F:9])[C:7]=1[F:8]

Participants

3

Reactant 2

HCID 27779433,4,5-TrifluorophenolHCID 19039101HCID 19039101, compound

Product 1

HCID 178461116HCID 178461116, compound

Procedure

The general procedure of Example 9 was repeated using 3,4,5-trifluorophenol and 4-bromomethyl-1-(4-fluoropentyl)-1-phenyl-1-silacyclohexane, thereby obtaining the intended compound.

Workup

  1. customobtaining the intended compound

Sources & evidence

ORD record
ord-ae804ec9190a42f29d49fc5d5ad86123
Source dataset
uspto-grants-1997_06
Patent number
US05641430

Reaction notes

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