1-Bromopentane → HCID 178447777, compound

HRID 1684463Notes

Reaction equation

HRID 1684463 reaction equation
[CH2:1](Br)[CH2:2][CH2:3][CH2:4][CH3:5].[Cl:7][C:8]1[CH:13]=[CH:12][C:11]([O:14][CH2:15][C@H:16]2[CH2:21][CH2:20][C@H:19]([CH:22]3[CH2:27][CH2:26][SiH:25](Cl)[CH2:24][CH2:23]3)[CH2:18][CH2:17]2)=[CH:10][CH:9]=1>>[Cl:7][C:8]1[CH:13]=[CH:12][C:11]([O:14][CH2:15][C@H:16]2[CH2:21][CH2:20][C@H:19]([C@H:22]3[CH2:27][CH2:26][Si@H:25]([CH2:1][CH2:2][CH2:3][CH2:4][CH3:5])[CH2:24][CH2:23]3)[CH2:18][CH2:17]2)=[CH:10][CH:9]=1

Participants

3

Reactant 2

HCID 80571-BromopentaneHCID 178478227HCID 178478227, compound

Product 1

HCID 178447777HCID 178447777, compound

Procedure

The general procedure of Example 30 was repeated using n-pentyl bromide and 4-(trans-4-(4-chlorophenyloxymethyl)cyclohexyl)-1-chloro-1-silacyclohexane, thereby obtaining the intended compound.

Workup

  1. customobtaining the intended compound

Sources & evidence

ORD record
ord-b853f788595d4be08a5d18a77c51557a
Source dataset
uspto-grants-1997_06
Patent number
US05641430

Reaction notes

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