HCID 19039054, compound → HCID 178444575, compound

HRID 1684465Notes

Reaction equation

HRID 1684465 reaction equation
[CH3:1][CH:2]([CH3:12])[CH2:3][CH2:4][CH:5]1[CH2:10][CH2:9][CH:8](Br)[CH2:7][CH2:6]1.[Cl:13][C:14]1[C:19]([F:20])=[CH:18][C:17]([O:21][CH2:22][CH:23]2[CH2:28][CH2:27][SiH:26](Cl)[CH2:25][CH2:24]2)=[CH:16][C:15]=1[F:30]>>[Cl:13][C:14]1[C:15]([F:30])=[CH:16][C:17]([O:21][CH2:22][C@H:23]2[CH2:24][CH2:25][Si@H:26]([C@H:8]3[CH2:9][CH2:10][C@H:5]([CH2:4][CH2:3][CH:2]([CH3:12])[CH3:1])[CH2:6][CH2:7]3)[CH2:27][CH2:28]2)=[CH:18][C:19]=1[F:20]

Participants

3

Reactant 2

HCID 19039054HCID 19039054, compoundHCID 123280316HCID 123280316, compound

Product 1

HCID 178444575HCID 178444575, compound

Procedure

The general procedure of Example 36 was repeated using 4-(3-methylbutyl)cyclohexyl bromide and 4-(4-chloro-3,5-difluorophenyloxyrnethyl)-1-chloro-1-silacyclohexane, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-a72b9d78b90f457a88fd205f83b3b993
Source dataset
uspto-grants-1997_06
Patent number
US05641430

Reaction notes

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