Potassium Carbonate → HCID 178460889, compound

Participants

Reaction Steps

8.3 g (60 mmols) of potassium carbonate was added to a mixture of 7.9 g (20 mmols) of 4-(trans-4-bromomethylcyclohexyl)-1-phenyl-1-n-propyl-1-silacyclohexane, 3.6 g (20 mmols) of 4-trifluoromethoxyphenol and 50 ml of dimethylformamide, followed by heating under reflux for 10 hours. The reaction mixture was after-treated by a usual manner and purified through chromatography to obtain 7.0 g (yield: 71%) of 4-(trans-4-(4-trifluoromethoxyphenyloxymethyl)cyclohexyl)-1-phenyl-1-n-propyl-1-silacyclohexane. The results of IR and NMR analyses are shown below.

Provenance & Evidence