3,4-Difluorophenol → HCID 178506030, compound

HRID 1684470Notes

Reaction equation

HRID 1684470 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[CH:6][C:7]=1[F:8].Br[CH2:11][C@H:12]1[CH2:17][CH2:16][C@H:15]([CH:18]2[CH2:23][CH2:22][Si:21](C3C=CC=CC=3)([CH2:24][CH2:25][CH2:26][CH2:27][F:28])[CH2:20][CH2:19]2)[CH2:14][CH2:13]1>>[F:1][C:2]1[CH:3]=[C:4]([O:9][CH2:11][C@H:12]2[CH2:13][CH2:14][C@H:15]([C@H:18]3[CH2:19][CH2:20][Si@H:21]([CH2:24][CH2:25][CH2:26][CH2:27][F:28])[CH2:22][CH2:23]3)[CH2:16][CH2:17]2)[CH:5]=[CH:6][C:7]=1[F:8]

Participants

3

Reactant 2

HCID 759273,4-DifluorophenolHCID 178506027HCID 178506027, compound

Product 1

HCID 178506030HCID 178506030, compound

Procedure

The general procedure of Example 39 was repeated using 3,4-difluorophenol and 4-(trans-4-bromomethylcyclohexyl)-1-phenyl-1-(4-fluorobutyl)-1-silacyclohexane, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-089221fc579d48a28441716428009e05
Source dataset
uspto-grants-1997_06
Patent number
US05641430

Reaction notes

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