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HRID1684580

反应详情

EQUATION

反应方程式

HRID 1684580 的结构方程式

REACTANTS

反应物

2
结构：O=C1CCC(=O)N1Br
HCID67184

1-Bromopyrrolidine-2,5-dione

C4H4BrNO2

结构：COc1ccc(-c2c(C(=O)CC(C)C)c(C)nc3cc(OC)c(OC)cc23)cc1OC
HCID19039903

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(-c2c(C(=O)CC(C)C)c(CBr)nc3cc(OC)c(OC)cc23)cc1OC
HCID19039900

未命名化合物

PROCEDURE

实验过程

According to the same manner as that described in Reference Example 5, 4-(3,4-dimethoxyphenyl)-3-isovaleryl-6,7-dimethoxy-2-methylquinoline was brominated with N-bromo-succinimide (NBS) to give 2-bromomethyl-4-(3,4-dimethoxyphenyl)-3-isovaleryl-6,7-dimethoxyquinoline. This compound was recrystallized from ethyl acetate - hexane to give colorless prisms. mp. 159°-161° C.